Chemistry (English) Preview
Bachelor	TR-NQF-HE: Level 6	QF-EHEA: First Cycle	EQF-LLL: Level 6

Course Introduction and Application Information

Course Code:

CHEM305

Course Name:

Organic Structure Analysis

Semester:

Fall

Course Credits:

ECTS

Language of instruction:

English

Course Condition:

Does the Course Require Work Experience?:

Type of course:

Compulsory Courses

Course Level:

Bachelor

TR-NQF-HE:6. Master`s Degree

QF-EHEA:First Cycle

EQF-LLL:6. Master`s Degree

Mode of Delivery:

Face to face

Course Coordinator:

Dr. Öğr. Üy. MELİKE ATAKOL

Course Lecturer(s):

Recep İşçi

Course Assistants:

Course Objective and Content

Course Objectives:

Knowledge of basic methods in organic structural determination, interpreting spectral data.

Course Content:

1. Short introduction to organic structure analysis. Elemental analysis.
2. UV Spectroscopy: Chromophore and auxochrome groups, electronic transitions, several examples from conjugated olefins, carbonyl compounds and aromatics.
3. IR Spectroscopy: Bond vibrational levels and functional groups, vibrational modes, CH, OH and NH bands, bands of major sp and sp2 hybridized functions, C-O and C-N bands.
4. Mass Spectrometry: Fragmentation patterns of molecules, effect of isotopes,
determination of the molecular mass.
5. NMR Spectroscopy: Nuclear spin and classification of nuclei, behavior in external magnetic field, basic concepts, chemical shift and its reasons, effect of alkyl groups, multiple bonds and magnetic anisotropy, spin-spin coupling and J values, long-range couplings, 1H and 13C NMR and examples for various chemical shifts and coupling constants

Learning Outcomes

The students who have succeeded in this course;
1) Elemental analysis and the use of the obtained data in structural determination
2) UV spectroscopy and the absorption spectra of the conjugated molecules
3) IR spectroscopy and its importance instructrural elucidation, bands of major functional groups
4) Mass spectrometry and its use in structural determination. Fragmentation patterns.
5) Basic concepts of NMR spectroscopy. Chemical shifts and spin-spin coupling
6) 1H NMR details and spectrum interpretation
7) Basic 13C NMR knowledge.

Course Flow Plan

Week	Subject	Related Preparation
1)	Elemental analysis. Introduction to spectroscopy. UV Spectroscopy
2)	UV Spectroscopy
3)	IR Spectroscopy
4)	IR Spectroscopy
5)	Examples of IR spectra
6)	Mass spectrometry
7)	Mass spectrometry
8)	Mass spectrometry
9)	NMR basic concepts, chemical shifts
10)	NMR chemical shifts, spin-spin couplings
11)	1H NMR in detail with solved problems
12)	1H NMR in detail with solved problems
13)	Basic 13C NMR
14)	Solved problems using all spectral data

Sources

Course Notes / Textbooks:	Organic Chemistry: Structure and Reactivity (5th Edition), Seyhan Eğe, Houghton-Mifflin 2003, ISBN 0618318097 (ISBN13: 9780618318094)
References:	1. Nükleer Manyetik Rezonans Spektroskopisi, Metin Balcı, METU Press - Ankara, 2000. 2. Spectrometric Identification of Organic Compounds, 8th Edition, 2014 Wiley; Robert M. Silverstein, Francis X. Webster, David J. Kiemle, David L. Bryce, ISBN: 978-0-470-61637-6

Course - Program Learning Outcome Relationship

Course Learning Outcomes	1	2	3	4	5	6	7
Program Outcomes
1) Knows the basic concepts related to the theory and applications of chemistry, uses theoretical and applied knowledge, can select, develop and design methods.
2) Makes experimental planning and application for analysis, synthesis, separation and purification methods, provide solutions to the problems encountered and interpret the results.
3) Expresses the basic principles of sample preparation techniques and instrumental analysis methods used in qualitative and quantitative analysis of items, discusses their application areas.
4) Has knowledge about the sources, production, industrial applications and technologies of chemical substances.
5) Makes structural analyzes of chemical substances and interprets the results.
6) Work individually and in multidisciplinary groups, take responsibility, plan their tasks and use time effectively.
7) Follows the information in the field and communicates with colleagues by using English at a professional level.
8) Uses information and communication technologies along with computer software at the level required by the field.
9) Follows the national and international chemistry literature, transfers the knowledge gained orally or in writing.
10) Determines self-learning needs, manages/directs his/her learning.
11) Takes responsibility and adheres to the ethical values required by these responsibilities.

Course - Learning Outcome Relationship

No Effect	1 Lowest	2 Average	3 Highest

	Program Outcomes	Level of Contribution
1)	Knows the basic concepts related to the theory and applications of chemistry, uses theoretical and applied knowledge, can select, develop and design methods.	2
2)	Makes experimental planning and application for analysis, synthesis, separation and purification methods, provide solutions to the problems encountered and interpret the results.	2
3)	Expresses the basic principles of sample preparation techniques and instrumental analysis methods used in qualitative and quantitative analysis of items, discusses their application areas.	2
4)	Has knowledge about the sources, production, industrial applications and technologies of chemical substances.
5)	Makes structural analyzes of chemical substances and interprets the results.	2
6)	Work individually and in multidisciplinary groups, take responsibility, plan their tasks and use time effectively.
7)	Follows the information in the field and communicates with colleagues by using English at a professional level.
8)	Uses information and communication technologies along with computer software at the level required by the field.
9)	Follows the national and international chemistry literature, transfers the knowledge gained orally or in writing.
10)	Determines self-learning needs, manages/directs his/her learning.
11)	Takes responsibility and adheres to the ethical values required by these responsibilities.

Assessment & Grading

Semester Requirements	Number of Activities	Level of Contribution
Midterms	1	% 40
Final	1	% 60
total		% 100
PERCENTAGE OF SEMESTER WORK		% 40
PERCENTAGE OF FINAL WORK		% 60
total		% 100

Workload and ECTS Credit Calculation

Activities	Number of Activities	Preparation for the Activity	Spent for the Activity Itself	Completing the Activity Requirements	Workload
Course Hours	13	3			39
Midterms	1	35			35
Final	1	50			50
Total Workload					124